Examinando por Materia "Plasma spraying"

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    Effect of the mechanical properties on drilling resistance of Al2O3-TiO2 coatings manufactured by atmospheric plasma spraying
    (ELSEVIER SCIENCE SA, 2013-04-15) Palacio, C. C.; Ageorges, H.; Vargas, F.; Diaz, A. F.; Universidad EAFIT. Departamento de Ciencias Básicas; Electromagnetismo Aplicado (Gema)
    Al2O3 with 13 and 45wt.% TiO2 microsized powders (6-22 and 13-41µm for each chemical composition) were used as raw materials to coat AISI 1040 steel by atmospheric plasma spraying. The mechanical properties of the coatings were measured by micro-indentation tests, and drilling experiments were carried out using high speed steel (HSS) rotary drill bits of various diameters and varying the load on the drill bits. In order to reduce the effect of the wear on the bit, a new bit was used for each test. According to the results, the drilling test is proposed as a method of determining the mechanical properties of these coatings from the correlation found between coating hardness and drilling resistance. © 2012 Elsevier B.V.
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    Study of APS and conventional sintering parameters for the manufacture of TiO2 targets for PAPVD
    (IOP PUBLISHING LTD, 2019-01-01) Jaramillo Raquejo D.; Palacio C.C.; Ageorges H.; Jaramillo Raquejo D.; Palacio C.C.; Ageorges H.; Universidad EAFIT. Departamento de Ciencias; Electromagnetismo Aplicado (Gema)
    In surface science of functional oxides, titanium dioxide (TiO2) is one of the most investigated crystalline systems either in rutile or anatase phases. In this work commercial TiO2 powders are used to study the required process conditions to obtain TiO2 targets by Atmospheric Plasma Spray (APS) and conventional sintering, with suitable physical and chemical properties to be source material for Plasma Assisted Physical Vapor Deposition (PAPVD) for technological and medical applications. Two three factor Box Behnken experimental designs combined with surface modeling were employed to estimate the influence of spraying parameters (gun current, Ar/H2 ratio and standoff distance) and sintering parameters (heating rate, sintering temperature and holding time) within the targets microstructure (cracks and pores in cross section) and phases composition. The microstructure and composition of APS-deposited targets and sintered ones were characterized by Scanning Electron Microscopy (SEM) and X-Ray Diffraction (XRD). The lowest defects percentages of the targets manufactured in this work were 0.41 ± 0.30 % for APS-deposited targets and 0.05 ± 0.04 % for the sintered ones using the optimal parameters suggested by the statistical model, which allowed confirming the advantages of sintering process and limitations of APS in terms of microstructural homogeneity, but also of the use of design of experiments in the modeling of systems of many variables when there is not diagnostic equipment of the processes available. © Published under licence by IOP Publishing Ltd.