Examinando por Materia "collagen"
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Ítem Contribution of Root Canal Treatment to the Fracture Resistance of Dentin(Elsevier Inc., 2019-01-01) Yan W.; Montoya C.; Øilo M.; Ossa A.; Paranjpe A.; Zhang H.; Arola D.D.; Yan W.; Montoya C.; Øilo M.; Ossa A.; Paranjpe A.; Zhang H.; Arola D.D.; Universidad EAFIT. Departamento de Ingeniería de Producción; Materiales de IngenieríaIntroduction: Although the strength and toughness of dentin decrease with age, no study has explored if restorative treatments are a contributing factor. Methods: Multiple extracted teeth were obtained from randomly selected donors and categorized according to donor age and prior root canal treatment. The microstructure and chemical composition of radicular dentin were evaluated using scanning electron microscopy and Raman spectroscopy, respectively, and the strength was evaluated in 4-point flexure to failure. Data were compared using the Student t test. Results: Dentin from the root canal–restored teeth exhibited significantly lower strength (P <.05) than tissue from age- and donor-matched unrestored tooth pairs. Although there was no significant difference in the mineral-to-collagen ratio between the 2 groups, dentin obtained from the root canal–treated teeth exhibited more extensive collagen cross-linking and lower tubule occlusion ratios than the unrestored tooth pairs. Conclusions: There is a decrease in the strength of radicular dentin with aging, but prior root canal treatment increases the extent of degradation. © 2018 American Association of EndodontistsÍtem Deformation behaviour of aged coronal dentin(Blackwell Munksgaard, 2018-06-01) Montoya; C.; Arola; D.; Ossa; E.A.; Universidad EAFIT. Departamento de Ingeniería de Producción; Materiales de IngenieríaObjective: This study aimed to identify the changes in the time-dependent deformation response of coronal dentin with ageing and its relationship with changes in chemical composition. Background: The structural behaviour of dentin with ageing is affected by changes in the density and diameter of its dentinal tubules (ie porosity), as well as changes in chemical composition throughout the tooth. However, little is known about the time-dependent deformation behaviour of aged dentin and the importance of its hierarchical structure and variations in chemical composition. Materials and methods: The spherical indentation response of aged coronal dentin was analysed in the outer, middle and inner regions, and its time-dependent deformation response was modelled in terms of its microstructure and chemical composition using a model recently proposed for young dentin. Results: The viscous deformation behaviour of aged dentin followed a power-law response with a decrease in the stress exponent when compared to young dentin. These results can be explained by cross-linking of the collagen present in the tissue. Conclusion: A decrease in the deformation ability of aged dentin was found. This behaviour could be a result of a dissolution process and reprecipitation of the minerals present in intertubular dentin into the dentinal tubules. © 2018 John Wiley & Sons A/S and The Gerodontology Association. Published by John Wiley & Sons LtdÍtem Effect of chemical composition and microstructure on the mechanical behavior of fish scales from Megalops Atlanticus(ELSEVIER SCIENCE BV, 2016-03-01) Gil-Duran, S.; Arola, D.; Ossa, E.A.; Gil-Duran, S.; Arola, D.; Ossa, E.A.; Universidad EAFIT. Departamento de Ingeniería de Producción; Materiales de IngenieríaThis paper presents an experimental study of the composition, microstructure and mechanical behavior of scales from the Megalops Atlanticus (Atlantic tarpon). The microstructure and composition were evaluated by Scanning Electron Microscopy (SEM) and RAMAN spectroscopy, respectively. The mechanical properties were evaluated in uniaxial tension as a function of position along the length of the fish (head, mid-length and tail). Results showed that the scales are composed of collagen and hydroxyapatite, and these constituents are distributed within three well-defined layers from the bottom to the top of the scale. The proportion of these layers with respect to the total scale thickness varies radially. The collagen fibers are arranged in plies with different orientations and with preferred orientation in the longitudinal direction of the fish. Results from the tensile tests showed that scales from Megalops Atlanticus exhibit variations in the elastic modulus as a function of body position. Additional testing performed with and without the highly mineralized top layers of the scale revealed that the mechanical behavior is anisotropic and that the highest strength was exhibited along the fish length. Furthermore, removing the top mineralized layers resulted in an increase in the tensile strength of the scale. © 2015 Elsevier Ltd.Ítem Reduction in Fracture Resistance of the Root with Aging(Elsevier Inc., 2017-09-01) Yan W.; Montoya C.; Øilo M.; Ossa A.; Paranjpe A.; Zhang H.; Arola D.; Yan W.; Montoya C.; Øilo M.; Ossa A.; Paranjpe A.; Zhang H.; Arola D.; Universidad EAFIT. Departamento de Ingeniería de Producción; Materiales de IngenieríaIntroduction: The incidence of vertical root fracture in endodontically treated teeth increases with patient age. This study evaluated the microstructure, chemical composition, and mechanical properties of radicular dentin as a function of aging. Methods: Single-rooted teeth were obtained from adult donors ranging from age 15 to older than 80 years. Beams were extracted from the middle third of the root and subjected to 4-point flexure to failure to evaluate strength of dentin in terms of donor age. Based on the strength distribution, the fatigue strength of root tissue from young (<= 30 years) and old (>= 55 years) donor teeth was evaluated via cyclic flexure loading. The microstructure and chemical composition of radicular dentin from the 2 groups were evaluated as a function of distance from the root apex using microscopy and Raman spectroscopy, respectively. Results: The strength decreased with age by approximately 25 MPa per decade, which resulted in a significant difference (P <= .0001) between the young (199 +/- 36 MPa) and old (122 +/- 11 MPa) groups. There was also a significant difference (P <= .0001) in fatigue strength between the young and old age groups. Both the mineral-to-collagen ratio and degree of cross-linking increased with age, with the largest changes identified in the apical and middle thirds, respectively. Conclusions: There is a reduction in the damage tolerance of radicular dentin with increasing age. This degradation appears to result from changes in the microstructure, corresponding chemical composition, and increase in collagen cross-linking with age, and is most severe near the root apex.Ítem Zylerberg, 1985 Contributions of the layer topology and mineral content to the elastic modulus and strength of fish scales(ELSEVIER SCIENCE BV, 2018-02-01) Murcia, S.; Miyamoto, Y.; Varma, M.P.; Ossa, A.; Arola, D.Fish scales are an interesting natural structural material and their functionality requires both flexibility and toughness. Our previous studies identified that there are spatial variations in the elastic properties of fish scales corresponding to the anatomical regions, and that they appear to be attributed to changes in the microstructure. In the present study, a model is proposed that describes the elastic behavior of elasmoid fish scales in terms of the relative contributions of the limiting layer and both the internal and external elasmodine. The mechanical properties of scales from the Megalops atlanticus (i.e. tarpon) were characterized in tension and compared with predictions from the model. The average error between the predicted and the experimental properties was 7%. It was found that the gradient in mineral content and aspect ratio of the apatite crystals in the limiting layer played the most important roles on the elastic modulus of the scales. Furthermore, misalignment of plies in the external elasmodine from the longitudinal direction was shown to reduce the elastic modulus significantly. This is one approach for modulating the fish scale flexibility for a high mineral content that is required to increase the resistance to puncture. © 2017